摘要介绍了3,4-二甲基苯胺的合成方法,采用催化加氢的方法合成3,4-二甲基苯胺。Introduced the synthetical methods of 3A-dimethylbenzenamine.Synthesized 3,4-dimethylbenzenamine by the method of catalytic hydrogenation.
4John F Knifton, Robert M Suggitt. Homogeneous ruthenium catalysts useful in the reduction of nitroaromatics to amines [ P ]. US :3832401,1974 - 08 - 24.
5John F Knifton, Robert M Suggitt. Homogeneous ruthenium catalysts useful in the selective reduction of nitroaromaties to amines[ P ]. US :3906045,1975 - 09 - 16.
6Chitta R Saha,Somnath Bhattacharya. Reduction of nitroaromatics with poly ( vinylpyridine ) complexes of palladium (Ⅱ) and platinum [ J ]. J Chem Tech Biotechnol, 1987,37:233 - 245.
7Liu B, Qiao M H, Deng J F,et al. Skeletal Ni catalyst prepared from a rapidly quenehed Ni-Al alloys and its high selectivity in 2 ethylanthraquinone hydrogenation[J]. J Catal, 2001,204 : 512 - 515.
8Hu H R,Xie F Z,Pei Y,et al. Skeletal Ni catalysts prepared from Ni-Al alloys rapidly quenched at different rates:texture, structure and catalytic performance in chemoselective hydrogenation of 2- ethylanthraquinone [ J ]. Journal of Catalysis ,2006,237 ( 1 ) : 143 - 151.
9Zhang H F,Wang A M,Li H,et al. Microstructure and catalytic properties of rapidly quenched Ni-A1-Cr-Fe alloy [ J ]. Material Letters ,2008,48 (6) : 347 - 350.
10Lei H,Song Z,Tan D L,et al. Preparation of novel Raney-Ni catalysts and characterization by XRD, SEM and XPS [ J]. Applied Catalysis A,2001,214( 1 ) :69 -76.
