甘氨酸合铜(Ⅱ)配合物的固、液相反应合成与表征

Synthesis and Characterization of (NH_2CH_2COO)_2 Cu(Ⅱ) by Solid-State and Liquid-State Reactions

以固相反应与液相反应两种方法合成了甘氨酸合铜(Ⅱ)配合物,研究了不同研磨时间对甘氨酸合铜(Ⅱ)配合物生成结果的影响。通过元素分析,红外光谱分析,紫外光谱分析,热重-差热等方法对产物进行了表征。实验结果表明,随着固相反应研磨时间的不同,对甘氨酸合铜(Ⅱ)配合物的生成结果有一定的影响,固、液相反应结果基本相同。

（NH2CH2COO）2 Cu（ Ⅱ ）was synthesized by solid-state and liquid-state reactions,and characterized by the EA, FT-IR, UV and TG-DTA techniques. The abrasing time in solid state reaction shows some effects on the final products. The products synthesized by solid-state and liquid-state reactions are identical.