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Synthesis and Crystal Structure of Tert-butyl 4-[(E)-4-(1,3-Dioxo-1,3-dihydro-2H-isoindol-2-yl)-1-butenyl] Benzoate

Synthesis and Crystal Structure of Tert-butyl 4-[(E)-4-(1,3-Dioxo-1,3-dihydro-2H-isoindol-2-yl)-1-butenyl] Benzoate
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摘要 The title compound tert-butyl 4-[(E)-4-(1,3-dioxo-1,3-dihydro-2H-isoindol-2-yl)- 1-butenyl] benzoate has been synthesized and characterized by X-ray crystallography. It crystallizes in monoclinic, space group C2/c with a = 14.875(3), b = 8.9796(13), c = 34.736(6) A°, β = 95.981(4)°, V= 4614.4(14)A°^3, Z= 8, Dc = 1.213 g/cm^3, F(000) = 1792,μ(MoKα) = 0.084 mm^-1, R = 0.0602 and wR = 0.1445 for 4613 unique reflections with 2272 observed ones (I〉 2σ(I)). The results of crystal structure determination show that the title compound has a layer structure, and the two benzene rings in molecule are parallel to each other. The title compound tert-butyl 4-[(E)-4-(1,3-dioxo-1,3-dihydro-2H-isoindol-2-yl)- 1-butenyl] benzoate has been synthesized and characterized by X-ray crystallography. It crystallizes in monoclinic, space group C2/c with a = 14.875(3), b = 8.9796(13), c = 34.736(6) A°, β = 95.981(4)°, V= 4614.4(14)A°^3, Z= 8, Dc = 1.213 g/cm^3, F(000) = 1792,μ(MoKα) = 0.084 mm^-1, R = 0.0602 and wR = 0.1445 for 4613 unique reflections with 2272 observed ones (I〉 2σ(I)). The results of crystal structure determination show that the title compound has a layer structure, and the two benzene rings in molecule are parallel to each other.
出处 《Chinese Journal of Structural Chemistry》 SCIE CAS CSCD 北大核心 2006年第3期300-304,共5页 结构化学(英文)
关键词 tert-butyl 4-[(E)-4-(1 3-dioxo-1 3-dihydro-2H-isoindol-2-yl)-1-butenyl]benzoate synthesis crystal structure tert-butyl 4-[(E)-4-(1,3-dioxo-1,3-dihydro-2H-isoindol-2-yl)-1-butenyl]benzoate, synthesis, crystal structure
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  • 1Sieval,A.B.; Linke,R.; Heij,G.; Meijer,G.; Zuilhof,H.; Sudholter,E.J.R.Langmuir.2001,17,7554-7559.
  • 2Xu,K.X.The Fine Chemical Raw Materials and Intermedia Handbook.Chemical Industry Press.Beijing 1998,P384-386.
  • 3Saroja,G.; Samanta,A.J.Chem.Soc.Faraday Trans.1996,92,2697-2701.
  • 4Takahashi,Y.; Yoshio,T.; Yamashita,H.; Kobayashi,S.; Ohno,M.Chem.Pharm.Bull.1986,34,2732-2742.
  • 5Sum,P.E.; Joseph,P.; Ziegler,C.B.US 4940710.1990-06-10.
  • 6Bhattacharyya,K.Acc.Chem.Res.2003,36,95-101.
  • 7Chen,Y.; Topp,M.R.J.Chem.Phys.Lett.2002,355,270-278.
  • 8Oberfield,J.L.; Collins,J.L.; Holmes,C.P.; Goreham,D.M.; Cooper,J.P.; Cobb,J.E.; Lenhard,J.M.;Hull-Ryde,E.A.; Mohr,C.P.Proc.Natl.Acad,Sci.U S A.1999,96,6102-6106.
  • 9Collins,J.L.; Holmes,C.P.; Lenhard,J.M.; Willson,T.M.WO 0027832.2000-05-18.
  • 10Siggins,J.E.; Ackerman,J.H.; Larsen,A.A.J.Med.Chem.1965,8,728-730.

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