摘要
以对硝基氯苯为原料,通过引入甲硫基后再进行置换、氟化制得对三氟甲硫基硝基苯;然后通过重氮化、水解得到目标产物对三氟甲硫基苯酚。总收率为56%。
Using 1-chloro-4-nitrobenzene as raw material, 1-nitro-4-（trifluoromethylthio） benzene was synthesized by introducing methylthio group and then via replacing fluorination. And then the title compound 4-[ （trifluoromethyl）thio]- phenol was obtained through diazotization and hydrolysis with total yield of 56%.
出处
《精细与专用化学品》
CAS
2006年第5期11-13,共3页
Fine and Specialty Chemicals
关键词
对硝基氯苯
重氮化
氟化
对三氟甲硫基苯酚
1 -chloro-4-nitrobenzene
diazotization
fluorination
4-[ （trifluoromethyl） thio ] -phenol
