摘要
This paper described a new method for preparation of ethyl lactate from ammonium lactate directly by means of reactive distillation in the presence of anhydrous aluminium chloride as catalyst and benzene as dehydrating agent.The result showed this method had the advantages of high pure,easy operation,and no pollution.The yield of ethyl lactate reached up to 28.14%,which was 50% higher 50% than that in ordinary reactive device.
This paper described a new method for preparation of ethyl lactate from ammonium lactate directly by means of reactive distillation in the presence of anhydrous aluminium chloride as catalyst and benzene as dehydrating agent. The result showed this method had the advantages of high pure,easy operation,and no pollution. The yield of ethyl lactate reached up to 28. 14% ,which was 50% higher 50% than that in ordinary reactive device.
出处
《化学研究与应用》
CAS
CSCD
北大核心
2006年第3期334-336,共3页
Chemical Research and Application
基金
国家自然科学基金重点资助项目(20036010)
河北省教育厅自然科学研究计划项目(2002150)
关键词
乳酸乙酯
乳酸铵
三氯化铝
反应精馏
enhyl lactate
ammonium lactate
aluminium chloride
reactive distillation