6-溴-2-己酮的合成

Chemical synthesis of 6-Bromo-2-hexanone

目的化学合成6-溴-2-己酮。方法以1,3-溴丙烷与乙酰乙酸乙酯为原料经环合、开环、溴代等反应合成。结果与结论目标产物的含量用GC方法测定含量95%以上,收率81.5%。

OBJECTIVE To synthesize 6-Bromo-2-hexanone. METHODS The compound was synthesized through the reaction of cyclization, split, bromination et al and using 1,3- propyl bromide and ethyl acetoacetate as raw materials. RESULTS and CONCLUSION The content of the compound determined by GC was 95% ,the recovery rate was 81.5%.