摘要
以硫酸钛为催化剂,利用微波辐射技术,在常压下肉桂酸与异戊醇合成肉桂酸异戊酯。实验表明,当n肉桂酸:n异戊醇:n硫酸钛=1:9:0.062时,采用800W微波80%火力辐射22.5min,肉桂酸异戊酯的产率达到83.9%。
Isoamyl cinnamate is syntheticed lastly with the technique of microwave radiation in the presence of titanium sulfate as a catalyst. They reacted with isoamyl alcohol and cinnamic acid under the normal pressure. The best reaction condition arc tile mole ratio of titanium sulfate , isoamyl alcohol and cinnamic acid is 1 : 9:0,062 . The power of miorwave is 640W, the radiating time of microwave is 22.5 min, the trasforming percentage may rcach 83.9%.
出处
《湖北师范学院学报(自然科学版)》
2006年第1期67-68,81,共3页
Journal of Hubei Normal University(Natural Science)