期刊文献+

D-72磺酸树脂催化合成(±)2-苯基-2-烷氧基乙醇 被引量:4

Catalytic Synthesis of(±)2-Phenyl2-alkyloxy-ethanol by Sulfuric Acid Resin D-72
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摘要 利用磺酸树脂D-72催化环氧苯乙烷与醇加成反应,合成了5种(±)2-苯基-2-烷氧基乙醇。其结构经1H NMR,IR和GC-MS表征。催化剂可重复使用8次。 Five ( ± )2-phenyl-2-alkyloxy-ethanols were synthesized via reactions of alcohol with styrene oxide using sulfuric acid resin D-72 as a catalyst. Thier structures were characterized by ^1H NMR, IR and GC-MS. Tha catalyst can be reused 8 times.
出处 《合成化学》 CAS CSCD 2006年第2期181-183,共3页 Chinese Journal of Synthetic Chemistry
基金 国家自然科学基金资助项目(29972011)
关键词 环氧苯乙烷 树脂 催化 合成 alcohol styrene oxide resin catalysis synthesis
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参考文献6

  • 1Fiorenza M,Ricci A,Taddei M,et al.Regiospecific conversion of oxiranes into primary alcohols via reaction with organotin derivatives[J].Synthesis,1983,(8):640-641.
  • 2Smith J G.Synthetically useful reactions of epoxides[J].Synthesis,1984:629-656.
  • 3Bonini C,Righi G.Regio-and chemoselective synthesis of halohydrins by cleavage of oxiranes with metal halides[J].Synthesis,1994:225-238.
  • 4Iranpoor N,Mohammadpour,Baltork I.Mild,efficient and selective opening of epoxides with alcohols catalyzed by ceric(Ⅳ) ammonium nitrate[J].Synth Commun,1990,20(18):2789-2797.
  • 5Taylor S K.Reactions of epoxides with ester,ketone and amide enolates[J].Tetrahedron,2000,56:1149-1163.
  • 6Mall T,Stamm H.Reactivity difference of cis-trans pairs:difference behavior of stilbene oxides and activated stilbene imines[J].J Org Chem,1987,52(21):4812-4814.

同被引文献31

  • 1胡云楚,刘元,孙汉洲,周莹,吴志平,袁光明.磷氮系膨胀型阻燃剂阻燃性能的热重分析[J].林产化学与工业,2005,25(1):61-65. 被引量:12
  • 2郭敏,卢建中.维生素B_1的分析方法概述[J].时珍国医国药,2006,17(7):1309-1311. 被引量:4
  • 3《全国原料药生产工艺汇编》编写组.全国原料药生产工艺汇编[M].上海:中国医药工业出版社,1980:620-622.
  • 4尹笃林,徐琼,毛丽秋,等.可再生植物原料制备固体磺酸的方法[P].CN:ZL200610032187.9,2008-10-01.
  • 5Xu Q. , Yang Z. G. , Yin D. L. , et al. Synthesis of chalcones catalyzed by a novel solid sulfonic acid from bamboo [J]. Catal. Commun. ,2008,9:1579-1582.
  • 6Xu Q. , Yang Z. G. , Yin D. L. One-pot three-component Mannich reaction catalyzed by sucrose char sulfonic acid [ J ]. Frontiers of Chemical Engineering in China. 2009, (1):1-5.
  • 7Firouzabadi H, Iranpoor N, Jafari A A, et al. Mluminumdodecatungstophosphate( AlPW13O40 )as a reusable Lewis acid catalyst:facile regioselective ring opening of epoxides with alcohols, acetic acid and thiols [J]. J. Mol. Catal. A- Chem. ,2006,250( 1-2 ) :237-242.
  • 8Chitwood H. C, freure B. The reaction of propylene oxide with alcohols [ J ]. J. Am. Chem. Soc., 1946,68 ( 4 ) : 680 -683.
  • 9Jaramillo C. , Chiara J L, Martin-Lomas M. An effective strategy for the synthesis of 6-O-(2-amino-2-deoxy-. alpha.-D-glucopyranosyl)-D-chiro- and -D-myo-inositol 1- phosphate related to putative insulin mimetics [ J ]. J. Org. Chem. , 1994,59( 11 ) :3135-3141.
  • 10Moberg C, Rakos L, Tottie L. Stereospecific Lewis acid catalyzed methanolysis of styrene oxide [J]. Tetrahedron Lett. , 1992,33(16) :2191-2194.

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