期刊文献+

平板玻璃受热后折射率的变化规律初探 被引量:4

Variation of the refractive indices of the plate glass after heat treatment
下载PDF
导出
摘要 目的探索平板玻璃受热后折射率的变化规律。方法首先采用差示扫描量热仪测定玻璃样品的转变温度Tg,将样品加热至不同的温度(温度范围从室温到Tg以上),自然冷却至室温后再用GRIM3测量折射率。结果加热温度在Tg以下时,玻璃的折射率基本不变,加热温度在Tg以上时,折射率有明显变化。结论对于从火灾和爆炸现场提取的玻璃,在进行折射率比对时应当考虑现场高温对测量值的影响,并进行必要的修正。 Objective To measure the plate glass refractive indices and find its changeable regularities after heat treatment. Methods Using DSC7 to measure the glass change temperature (Tg), heat the specimen to different degree (from room temperature to Tg up ) , after natural cooling-off, then using GRIM3 equipment to measure the refractive index. Results The effects of low temperature (below Tg) to glass refractive indices can been seen as zero, that of high temperature (above Tg) is very critical. Conclusion We must think over the effects of the temperature at scene when using the refractive indices to identify the glass recovered from fire scene.
出处 《刑事技术》 2006年第2期11-14,共4页 Forensic Science and Technology
关键词 折射率 玻璃化转变温度Tg 匹配温度 refractive index glass change temperature match temperature
  • 相关文献

参考文献8

  • 1[1]权养科,陶克明,冯计民,等.玻璃物证系统检验方法研究[C].第四届全国微量物证检验学术交流会论文汇编,1999,133-136.
  • 2[2]张玉智,唐炳文,蒋爱生.玻璃的退火和钢化[M].中国建筑工业出版社,1989,51-59.
  • 3[3]千福熹.现代玻璃科学技术(上册)[M].上海科学技术出版社,1988,104-115.
  • 4[4]谢于深.玻璃化学[M].轻工业出版社,1988,97-131.
  • 5[5]Warman G P,Keeley R H.An introduction to glass technology[J].Metropolitan Police Forensic Science Laboratory Report No.30,1983:1-12.
  • 6[6]Edmondstone G.The identification of heat strengthened glass in windshields[J].Can.Soc.Forens.Sci.J.1997,30:181-184.
  • 7[7]Cassista A R,Sandercock P M L.Precision of glass refractive index measurements:temperature variation and double variation methods,and the value of dispersion[J].Can.Soc.Forens.Sci.J.1994,27:203-207.
  • 8[8]Cassista A R,Sandercock P M L.Effects of annealing on toughened and nontoughened glass[J].Can.Soc.Forens.Sci.J.1994,27:171-176.

同被引文献29

  • 1唐可娜,曾途,罗凯.玻璃微量物证检验在案件证据链中的联接作用[J].广西警官高等专科学校学报,2007,20(S1):11-13. 被引量:1
  • 2姜红.刑事案件现场中微量玻璃的检验及应用[J].玻璃与搪瓷,2005,33(1):43-46. 被引量:3
  • 3K. Walsh, J. S. Buckleton, C. M. Triggs. A practical exam-pie of the interpretation of glass evidence[J]. Science & Justice, 1996, 36(4): 213-218.
  • 4Y. Suzuki, R. Sugita, S. Suzuki, Y. Marumo. Forensic Dis- crimination of bottle glass by refractive index measurement and analysis of trace elements with ICP-MS[J]. Analytical Sciences, 2003, 16:1195-2000.
  • 5国家标准GB7962.11987《无色光学玻璃测试方法折射率和色散系数测试方法》[S].
  • 6国家标准GB/T7962.11-1987《无色光学玻璃测试方法折射率精密测试方法》[S].
  • 7J. Locke.GRIM: A semi-automatic device for measuring the refractive index of glass particles [J]. Microscope, 1985, 33 (3): 169-178.
  • 8ASTM International. ASTM E1967-98. Standard test method for the automated determination of refractive index of glass sam- pies using the oil immersion method and a phase contrast micro- scope. West Conshohken, PA: ASTM International, 2003.
  • 9廖然,马辉,何永红.一种折射率色散特性的检测系统及其检验方法[P].国家发明专利,专利号:ZL200910108706.9.
  • 10权养科,陶克明,冯计民.热台相差显微镜法测定平板玻璃的折射率[J].刑事技术,1997,22(6):1-3. 被引量:3

引证文献4

二级引证文献6

相关作者

内容加载中请稍等...

相关机构

内容加载中请稍等...

相关主题

内容加载中请稍等...

浏览历史

内容加载中请稍等...
;
使用帮助 返回顶部