一种含硅的三氮唑衍生物的合成研究
Synthesis Research of 2-(2,4-Difluorophenyl)-1-(1H-1,2,4-Triazol-1-yl)-3-Trimethylsilyl-2-Propanol
摘要
对一种新型的杀菌剂———含硅的三氮唑衍生物的合成进行了改进,并给出了一条新的合成路线.以化合物1为起始原料通过付克反应、格氏反应和取代反应,得到最终产物化合物5.改进后的工艺操作更方便,收率达46%.
A new process for preparing the new fungicide-silicon-containing triazole derivative is described. Compound 5 is synthesized through Frieldel-Crafts reaction, Grignard reaction and substitution reaction from compound 1 which serves as starting materials. The total yield is 46 %.
出处
《同济大学学报（自然科学版）》
EI
CAS
CSCD
北大核心
2006年第4期549-551,共3页
Journal of Tongji University:Natural Science
基金
国家自然科学基金资助项目(29971023)
关键词
含硅的三氮唑衍生物
杀菌剂
合成
silicon-containing triazole derivative
fungicide
synthesis
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