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热喷雾进样火焰原子吸收光谱法测定河水中的铅 被引量:5

Determinaion of lead by thermospray flame-heated quartz tube atomic absorption spectrometry
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摘要 A flame-heated puartz tube was utilized as an atomzer for atomic absorption spectrometric determination of lead with thermospary sampling.Under optimal conditions,a sensitivity enhancement factor of 92 was obtained in comparison with that of conventional flame atomic absorption spectrometry.Detection limits for lead was 3ng/mL compared with 80ng/mL by conventional flame atomic absorption spectrometry.The proposed method was applied for the determination of trace lead in a river water sample with recovery of 96-102%. Atlame - heated puartz tube was utilized as an atomzer for atomic absorption spectrometric determination of lead with thermospary sampling. Under optimal conditions, a sensitivity enhancement factor of 92 was obtained in comparison with that of conventional flame atomic absorption spectrometry. Detection limits for lead was 3ng/mL compared with 80ng/mL by conventional flame atomic absorption spectrometry. The proposed method was applied for the determination of trace lead in a river water sample with recovery of 96 - 102%.
出处 《化学研究与应用》 CAS CSCD 北大核心 2006年第5期576-578,共3页 Chemical Research and Application
关键词 热喷雾 石英管 原子吸收 河水 thermospary quartz tube atomic absorption spectrometry lead river water
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