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Controlled Synthesis and Electrochemical Behavior of Single-crystal MoO_2 Nanowhiskers by a Facile Precursor-reduction Route

Controlled Synthesis and Electrochemical Behavior of Single-crystal MoO_2 Nanowhiskers by a Facile Precursor-reduction Route
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摘要 A novel method for controlled synthesis of crystalline molybdenum dioxides nanowhiskers (whisker-MoO2) by using moderate reductive and precursor ion under hydrothermal conditions is reported. The result shows that the as-obtained samples have a monoclinic structure, and the whisker-MoO2 is composed of nanowires with diameters of ca. 20 nm. Formation of whisker-MoO2 was through a typical precursor-reduction process, in which cetyltrimethylammonium bromide (CTAB) served as a cationic surfactant and acetone as a reductant. The electrochemical behavior of whisker-MoO2 was studied. A novel method for controlled synthesis of crystalline molybdenum dioxides nanowhiskers (whisker-MoO2) by using moderate reductive and precursor ion under hydrothermal conditions is reported. The result shows that the as-obtained samples have a monoclinic structure, and the whisker-MoO2 is composed of nanowires with diameters of ca. 20 nm. Formation of whisker-MoO2 was through a typical precursor-reduction process, in which cetyltrimethylammonium bromide (CTAB) served as a cationic surfactant and acetone as a reductant. The electrochemical behavior of whisker-MoO2 was studied.
出处 《Chinese Chemical Letters》 SCIE CAS CSCD 2006年第6期825-828,共4页 中国化学快报(英文版)
基金 This work was financially supported by the National Natural Science Foundation of China (No.20271001).
关键词 Synthetic methods characterization MoO2 nanowhiskers electrochemical behavior. Synthetic methods, characterization, MoO2 nanowhiskers, electrochemical behavior.
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