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四氧化二氮中相当水含量的分析检测方法 被引量:9

Analysis methods to determine equivalent water content in nitrogen tetroxide
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摘要 四氧化二氮和加入一定比例一氧化氮的四氧化二氮是非常重要的火箭推进剂,相当水含量是其最重要的一项技术指标。本文对四氧化二氮中相当水含量的分析检测方法包括气相色谱法、近红外光谱法、微波法、核磁共振法等分别进行介绍,并重点介绍核磁共振法的原理及其应用。 Nitrogen tetroxide and nitrogen tetroxide that contained certain proportional nitrogen oxide are the important rocket propellants, and the equivalent water content is one of the most important technique index. The analysis methods to determine the'equivalent water content in nitrogen tetroxide are introduced in this paper, including gas chromatography method, near-infrared spectra method, microwave method and NMR method. The theory and the application of NMR method is emphasized in the paper.
出处 《现代仪器》 2006年第3期8-10,共3页 Modern Instruments
关键词 四氧化二氮 相当水 核磁共振 Nitrogen tetroxide Equivalent water NMR
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参考文献8

  • 1Military Specification,Propellants,Nitrogen Tetroxide,MIL-P-26539C,1976
  • 2Military Specification,Propellants,Nitrogen Tetroxide,MIL-P-26539D,1989
  • 3GJB 1673-93,四氧化二氮规范
  • 4GJB 1964-94,绿色四氧化二氮规范
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  • 7Vango S.P.and Manatt S.L.Nuclear magnetic resonance determination of water and oxygen titration for nitric oxide in liquid nitrogen tetroxide.Anal.Chem.,1973,45:1060
  • 8Dove M.F.A.,Logan N and Wood S.A.,Determination of trace of water in NTO/MON by FT proton NMR spectrometry.AIAA-93-2039

同被引文献38

  • 1刘再华,刘艳英.绿色四氧化二氮相当水含量超标分析[J].导弹与航天运载技术,2004(4):57-62. 被引量:6
  • 2程志梅,信聪,张勇.WSJBQ-005型水红外分析仪的改进[J].计测技术,2005,25(B06):60-62. 被引量:2
  • 3王菊香,邢志娜,申刚.液体推进剂质量分析发展综述[J].化学推进剂与高分子材料,2007,5(2):37-39. 被引量:3
  • 4MIL-P-26539C, Military Specification, Propellants, Nitrogen Yetroxide[S]. 1976.
  • 5MIL-P-26539D, Military Specification, Propellants, Nitrogen Tetroxide[S]. 1989.
  • 6GJB1673-1993,四氧化二氮规范[S].
  • 7GJB1964-1994,绿色四氧化二氮规范[S].
  • 8VANGO S P, MANATT S L. Nuclear magnetic resonance determination of water and oxygen titration for nitric oxide in liquid nitrogen tetroxide [J]. Anal Chem, 1973 , 45 :1060-1064.
  • 9GEORGE A W. Applications of NMR in quantitative analysis[J]. American Laboratory, 1970,5 : 12-26.
  • 10DOVE M F A, LOGAN N, WOOD S A. Determination of trace of water in NTO/MON by FT proton NMR spectrometry[C]. AIAA. 29^th joint propulsion conference and exhibit. Monterey: AIAA, 1993: 28- 30.

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