摘要
研究了用微波消解法分解润滑脂并用ICP—AES测定硼的方法，确定了合适的微波消解条件，优化了ICP—AES的工作参数，消除了共存元素的干扰。本方法的回收率为94％-105％，相对标准偏差≤5．08％（11=8）。
It is researched the method of boron determination by ICP - AES using microwave digestion method to decompose lubricating grease, the proper conditions of microwave digestion are settled down, the working parameters of ICP - AES are optimized, and the interference of co - existent elements is eliminated. The recovery of this method is 94% -105%, and the relative standard derivation is ≤5.08% （n = 8）
出处
《合成润滑材料》
CAS
2006年第2期10-16,共7页
Synthetic Lubricants
关键词
ICP—AES
微波消解
硼
润滑脂
ICP - AES
microwave digestion
boron
lubricating grease
