摘要
纳米氧化锌的合成与表征何勇宁,沈孝良,马礼敦(复旦大学分析测试中心上海200433)关键词纳米材料,氧化锌,合成,表征制备纳米材料的方法很多,如蒸发冷凝法、化学气相沉积法、溶胶-凝胶法、超临界法、水热法及各种热分解法等。Liu等[2]用超声雾化热分解...
Nanometer-sized zinc oxide was synthesized by five different procedures without any surface activating agents. Their structures were characterized by X-ray powder diffraction,transmission electron microscope,infrared spectroscopy and extended X-ray absorption fine structure. The shape of ZnO grains is spheric and their diameter ranges from 10 nm to 80 nm. The influences of synthesis type,reaction conditions,processing procedures of inter mediates, thermodecomposition conditions on the grain size were discussed.
出处
《应用化学》
CAS
CSCD
北大核心
1996年第4期92-94,共3页
Chinese Journal of Applied Chemistry
关键词
纳米材料
氧化锌
合成
nanometer-sized material
zinc oxide
synthesis
characterization