摘要
用电感耦合等离子体质谱法(ICP—MS)测定了5个黄沙原土样品中铅同位素比207Pb/206Pb、208Pb/206Pb,样品来自被认为是黄沙气溶胶源地区,为了使铅同位素测量中质量偏差和漂移减至最少,在样品中加入了铊标准溶液,测量205Tl/203Tl比,校正质量数差别选择的影响.同时,采用ICP—MS和电感耦合等离子体原子发射光谱法(ICP一AlS)测定了随粒径变化样品中12种元素浓度的变化.
Five original KOSA soils,collected in the locations of being thought to be the origins of KOSA aerosol in China,were analyzed by inductively coupled plasma mass spectrometry (ICP-MS) to determine the lead isotope ratios 207Pb/206Pb and 208Pb/206Pb.Tominimize mass bias and drift in Pb isotope measurement,the mass discrimination correction,based upon the addition of thallium to the samples and measurement of 205Tl/203Tl ratio,was used.At the same the, concentrations of 12 elments were determined as a function of particle-size by ICP-MS and induedvely coupled plasma atomic emission spectrometry (ICP-AES).
出处
《分析测试技术与仪器》
1996年第2期8-14,共7页
Analysis and Testing Technology and Instruments
关键词
铅分析
同位素比
黄沙
土壤分析
Isotope ratio Original KOSA soil Inductively coupled plasma mass spectrometry Inductively coupled plasma atomic emission spectrometry Soil analysis