摘要
以(NH4)6Mo7O24.4H2O,NiSO4.6H2O,(NH4)2S2O8为原料合成了(NH4)6[NiMo9O32].8H2O(九钼镍杂多酸铵),利用化学分析、差热热重、红外光谱、紫外光谱等方法对其进行了元素分析及结构的表征.
Ammonium 9-molybdate nickel heteropoly salt with Waugh structure was synthesized by the reaction of nickel sulfate and ammonium heptamolybdate by oxidation of ammonium peroxydisulfate. The ultimate analysis and the structure were characterized by IR, UV-Vis, TG-DTA thermal analysis and chemical analysis.
出处
《河北师范大学学报（自然科学版）》
CAS
北大核心
2006年第4期443-445,共3页
Journal of Hebei Normal University：Natural Science
关键词
WAUGH结构
九钼镍杂多酸铵
合成
表征
Waugh structure
ammonium 9-molybdate nickel heteropoly salt
synthesis
characterization
