摘要
本文研究了在室温下微波催化合成二糠叉环己酮的优化工艺条件。结果表明:糠醛与环己酮摩尔比2:1,功率为320W,反应2分钟时,二糠叉环己酮的产率最大,可达90.2%。
Synthesis of difurfurylidene cyclohexanone by microwave irradiation at room temperature was studied. The results demonstrated that with microwave power of 320 W for 2 min when the mole ratio of furfural: cyclohexanone was 2 : 1 , the yield of n - butyl benzoate reached 90.2 %.
出处
《南平师专学报》
2006年第2期30-33,共4页
Journal of Nanping Teachers College
关键词
微波
正交实验
合成
二糠叉环己酮
microwave orthogonal test synthesis difurfurylidene cyclohexanone