摘要
本文介绍了一种活性深蓝的新的合成方法,通过住酸性偶反应中添加助剂,改善反应的流动性,并使反应更完全;同时采用对位酯一缩,间苯二胺的二缩的新工艺,进一步提高了产物的固色率,并大大提高了产物的收率,大幅降低产品成本。
In this paper ,we introduced a new method of synthesis for a reactive blue dye .We used an auxiliary in the acid coupling reaction to reduce the viscosity of the solution. Then cyanuric chloride reacted with 4- (-sulfatoethylsulfonyl) aniline, and 2,4-diamino benzensulfonate. They made the reactions more completely. The title dye is prepared in high yield and high fixation than reported. The price of the production is lower than ever.
出处
《上海染料》
2006年第4期18-21,共4页
Shanghai Dyestuffs
关键词
助剂
缩合反应
偶合反应
Auxiliary
Condensing reaction: Coupling reaction