摘要
以氯铂酸－胺体系为催化剂的硅氢加成法合成甲基（γ－氯丙基）二氯硅烷，考察了反应温度、原料配比、催化剂用量、反应时间等因素对反应产物收率的影响，选择出最佳工艺条件，硅氢加成收率达到８１％．
Methyl(γ chloropropyl)dichlorosilane was prepared by using the catalyzing of platium amine for the catalyzing hydrosilation of methyldichlorosilane with 3-chloro propene.The effect of various possible facts and the reaction conditions on the results was also investigated.It was found that the catalyst has high activity under 20/10 6.The product is obtained in 81% yield.
出处
《江西师范大学学报（自然科学版）》
CAS
1996年第4期294-298,共5页
Journal of Jiangxi Normal University(Natural Science Edition)
基金
江西省重点攻关项目
关键词
甲基二氯硅烷
烯丙基氯
制备
工艺
hydrosilation,chloropropene methyldichloro silane,choroplatinic
