超增溶自组装制备纳米氧化镍

Preparation of nanoparticle nickel oxide by supersolubilizing self-assembly

采用超增溶自组装合成了纳米氧化镍，并通过透射电镜（TEM）、X射线衍射（XRD）、N2吸附脱附BET法和热重分析（TG）表征了其结构。结果表明，形成的纳米粒子分散性良好，粒径分布较窄（10-20nm），晶粒度良好，微晶晶化比较完全，氧化镍纳米粒子具有较大的孔径，比表面积和孔容符合纳米粒子特性。确定了超增溶自组装制备纳米氧化镍的最佳工艺条件。

Nanoparticle nickel oxide was prepared by supersolubility self-assemblycharacterized by means of X-ray powder diffraction （ XRD ）, transmission electron microscopy （ TEM ）, thermogravimetry （TG） and N2 adsorption. The results indicated that the nanoparticle nickel oxide particles were well-dispersed, with narrow distribution of particle size（ 10 - 20 nm）, good crystallinity, well-crystallized microcrystals, larger pore size and surface area and pore volume conforming to characteristics of nanoparticles. The optimum conditions for preparation of NiO nanoparticles were determined through experiment.