摘要
提出一种以间甲苯胺为原料,在铜盐催化室温条件下,经重氮盐制备间甲苯酚的简单方法。利用正交试验法设计实验方案,对实验结果进行统计分析,选择最佳反应条件,该方法条件缓和,反应迅速,操作简便,产率达90%以上。
A simple method for preparing m -cresol from m -toluidine via diazonium salt at room temperature using copper salt as a catalyst is proposed. The orthogonal test was applied to design the experiment and the statistical analysis of the result was made, the reaction condition being optimized. The method has a characteritics of moterate reaction condition, operating easily and high yield.
出处
《抚顺石油学院学报》
1996年第4期26-27,30,共3页
Journal of Fushun Petroleum Institute
关键词
重氮盐
正交试验
铜盐催化剂
间甲苯酚
Diazonium salt
Orthogonal test
Copper salt catalyst
m -Cresol