摘要
采用连续浸提法将硼泥中的硼划分为七种物理形态,即:水溶态、醇溶态、盐溶态、络合态、硫酸盐等结合态、Fe-Mn结合态及残渣态。用分光光度法测定各形态硼的含量。测定结果的相对标准偏差为4.4%(n=4),回收率为91.7%~102.4%。
The sequential chemica sludge combin into seven fractions; wate ed and residual speci spectrophotometry. The RSD 1 extractions have been developed for partitioning of boron in the boron r soluble, ethanol soluble, salt soluble, chelate, sulfate combined, Fe-Mn es. The content of boron in different fractions was determined by was 4.4%(n=4),and the recovery was 91.7%-102.4%.
出处
《分析科学学报》
CAS
CSCD
2006年第5期555-558,共4页
Journal of Analytical Science
关键词
连续浸提法
硼泥
形态分析
分光光度法
Sequential chemical extractions
Boron sludge
Speciations
Spectrophotometry