一个带羟基的C_（60）吡咯烷衍生物的合成与表征

Synthesis and Characterization of a [60]Fulleropyrrolidine with a Hydroxyl Group

氮气流保护下，Ｃ６０与聚甲醇和苏氨酸在干燥的甲苯中反应生成一个带羟基的Ｃ６０。吡咯烷衍生物。标题化合物用ＦＤ－ＭＳ，ＦＴ－ＩＲ，ＵＶ－ＶＩＳ和１Ｈ－ＮＭＲ进行了表征。

A [60]fulleropyrrolidine with a hydroxyl group was obtained from the 1, 3 dipolar cycloaddition reaCtion of C60 and a azomethine ylide generated iap situ from heating paraformaldehyde and DL - threonine in dry toluene. The Structure of the title compound was assigned on the basis of FD - MS, FT - IR, UV - Vis and 1H - NMR spectroscopy.