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牛奶中土霉素、金霉素的残留分析方法研究 被引量:3

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摘要 运用反相高效液相色谱-二极管阵列检测器建立了牛奶中土霉素、金霉素的残留分析方法。柱子采用Waters Nova-park C18柱(4μm,3·9mm i·d·×150mm),以体积比为68∶12∶20的0·01mol/L草酸溶液-乙腈-甲醇作为流动相,流速为1·0mL/min,柱温为30℃,检测波长为360nm,在上述色谱条件下,土霉素、金霉素在10min内得到了有效的分离和检测。建立的方法简便、快捷、线性范围宽,可用于牛奶中土霉素、金霉素的残留量分析。
出处 《云南畜牧兽医》 2006年第5期37-38,共2页
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参考文献4

  • 1Residues of some veterinary drugs in animal and foods[Z]. 38^th meeting of the joint FAO/WHO Expert Committee on Food Additives , Food and Agriculture Organized of the United Nations,Rome. FAO Food and Nutrition Papers. 1991.
  • 2中华人民共和国农业部第235号公告.动物性食品最高残留限量[S].2002.
  • 3Austin R L, Loly C H, Malbrough, et al. Matrix Slhd - Phase dispersion (MSPD) Isolation and liquid chromatograph determination of oxytetracycline, tetracycline , and chlortetracline in milk[ J ]. AOAC Int, 1990,73 (3) :379 - 384.
  • 4张素霞,李俊锁,钱传范.牛奶中四环素类药物多残留分析方法研究——MSPD-HPLC-UV[J].畜牧兽医学报,2002,33(1):51-54. 被引量:40

二级参考文献10

  • 1Korsrud G O,Boison J O,Nouws J D,et al.Bacterial inhibition tests used to screen for antimicrobial veterinary drug residues in slaughtered animals[].Journal of AOAC International.1998
  • 2Chao L C,Xuelin G.Determination of tetracycline residues in bovine milk, serum, and urine by capillary electrophoresis[].Journal of AOAC International.1995
  • 3Austin R L,Lily C H,Malbrough,et al.Matrix SolidPhase dispersion ( MSPD ) Isolation and liquid chromatographic determination of oxytetracycline, tetracycline, and chlortetracycline in milk[].Journal of AOAC International.1990
  • 4Ashworth R B.Liquid chromatographic assay of tetracyclines in tissues of food- producing animals[].Journal of AOAC International.1985
  • 5Tyczkowska K,Aronson A L.Simultaneous liquid chromatographic determination of some tetracyclines in serum[].Journal of AOAC International.1986
  • 6Okra H,Ikai Y,Kawamura J,et al.Photodecomposition produets of tetracycline in qaueous solution[].Journal of Agricultural and Food Chemistry.1989
  • 7HisaoO,YoshitomoI,JunkoH.ImprovementofchemicalanalysisofantibioticsPartXIX:Determinationoftetracyclineantibioticsinmilkbyliquidchromatographyandthin-layerchromatographyfastatombombardmentmassspectrometry[].JAOACInt.1994
  • 8Jeffery R M,Guy R S,William H G.Liquid Chromatographic determination of oxytetracycline in edible fish fillets from six species of fish[].Journal of AOAC International.1998
  • 9WhiteCR,MoatsWA,KotulaKL.OptimizationofaliquidChromatographicmethodfordeterminationofoxytetracycline,tetracycline,andchlortetracyclineinmilk[].JAOACInt.1993
  • 10Carson M C,Breslyn W.Simultaneous determination of multiple tetracycline residues in milk by metal chelate affinity chromatography: collaborative study[].Journal of AOAC International.1996

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