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固相微萃取/气-质联机分析荆条叶、枝的头香香气 被引量:9

Analysis of aroma from leaf and stem of vitex negundo l.var. heterophylla (franch.) rehd.by solid phase microextraction combing with GC-MS
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摘要 顶空固相微萃取/气相色谱-质谱方法分析了北京地区芳香植物荆条叶、枝的头香香气组成,采用计算机质谱谱库检索结合气相色谱保留指数的二维定性方法,从荆条叶中鉴定出36种挥发性成分,质量分数92.72%;从荆条枝中鉴定出33种挥发性成分,质量分数97.30%。所鉴定出组分多数为单萜及倍半萜类化合物,在荆条叶、枝中含量最高的均为β-丁香烯、其次为香桧烯、1,8-桉叶素、对-聚伞花烃等。 The aroma from leaf and stem of the fragrant plant, Vitex negundo L.var. heterophylla(Franch.)Rehd. occuring in Beijing area,was analyzed by gas chromatography-mass spectrometry combining with headspace solid phase microextraction. Through comparison with mass spectra database and their retention indices relative to n-alkanes, thirty-six components from the leaf and thirty-three components from the stem were identified, covering 92.72% and 97.30 % of the total peak areas in the GC-MS total ion current chromatography respectively. Both the leaf and the stem aroma were composed mainly of monoterpene and sesquiterpene constituents, with β-caryophyllene the most major, followed by sabinene, 1,8-cineole, p-cymene ect.
出处 《食品科技》 CAS 北大核心 2006年第10期260-263,共4页 Food Science and Technology
基金 北京市优秀人才培养资助项目(20051D0500310)
关键词 荆条 固相微萃取 香气组成 β-丁香烯 香桧烯 1 8-桉叶素 对-聚伞花烃 Vitex negundo L.var. heterophylla(Franch.)Rehd Solid phase extraction Aroma constituents β- Caryophyllene Sabinene 1,8-Cineole p-Cymene
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  • 1方洪钜,陈鹭声,周同惠.挥发油成分的研究——Ⅲ.腋花杜鹃挥发油的化学成分研究和牡荆、荆条挥发油成分的比较[J]药学学报,1980(05).

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