摘要
用异辛酸为原料，经过同氢氧化钠皂化和氯化铈复分解反应，合成了异辛酸铈，研究了皂化率、反应时间、反应温度对氯化铈转化率的影响。实验得到了最佳工艺条件：反应时间20min左右、温度55～65℃、皂化率为75％，氯化铈的转化率可达到99．996％以上。
The drier cerium isooctanoate has been prepared using isooctanoate as raw material by means of sodium hydroxide saponification and cerium chloride decomposition reaction. The influence factors of conversation ratio such as saponification ratio,reaction time and temperature were investigated. The optimum conditions were obtained： reaction time is about 20 min,temperature is 55 ℃ ～65 ℃ ,saponification ratio is 75 %, conversation ratio is above 99. 996 %.
出处
《化工科技》
CAS
2006年第5期8-10,共3页
Science & Technology in Chemical Industry
基金
2002年抚顺市科技局科学研究计划项目(20020114)
关键词
异辛酸铈
合成
氯化铈
Cerium isooctanoate
Synthesis
Cerium chloride
