摘要
利用微波辐射催化芳香醛与绕丹宁乙酸的缩合反应,合成了10个5-亚苄基绕丹宁乙酸衍生物,反应时间8—20min,产率良好,操作简便。
The 5-arylmethylidene rhodanine acetic acid derivatives were synthesized by the condensation of rhodanine acetic acid with aromatic aldehyde in sodium acetate/acetic acid under microwave irradiation. This method had some advantages such as better yields, shorter reaction time and milder reaction conditions.
出处
《化学试剂》
CAS
CSCD
北大核心
2006年第11期668-670,共3页
Chemical Reagents
基金
国家自然科学基金(20571029)
江苏省低维材料化学重点建设实验室开放基金(JSKC05021)资助。
关键词
微波辐射
绕丹宁乙酸
缩合
芳醛
microwave irradiation
rhodanine acetic acid
condensation
aromatic aldehyde