摘要
为研究消毒产品中三氯生含量测定方法,采用高效液相色谱法进行了实验室观察.结果,经过波长扫描选择最佳测定波长为281 nm,流动相选择甲醇与水比例4：1可达到较好的分离效果.该方法最低检出浓度为1 μg/ml;方法的线性范围为0.01～0.8 mg/ml;平均回收率为100.2%,相对标准偏差＜10%.结论,用高效液相色谱法检测消毒产品中三氯生含量,方法简便、精确.
In order to study the method for measuring triclosan content in disinfection products, high performance liquid chromatography （HPLC） was used to carry out laboratory observation. Results： By wavelength scanning, the best measuring wavelength selected was 281 nm and the mobile phase selected was methanol：water =4 ： 1. With these conditions, good separation efficacy could be achieved. The lowest concentration detected by this method was 1 μg/ml. The linear range of the standard curve was 0.01 -0.8 mg/ml, the average recovery rate was 100.2% and the relative standard deviation was 〈 10%. Conclusion： Measuring triclosan content in disinfection products by HPLC is simple, convenient and accurate.
出处
《中国消毒学杂志》
CAS
北大核心
2006年第6期551-552,共2页
Chinese Journal of Disinfection
关键词
消毒产品
三氯新
高效液相色谱法
检测
disinfection product
triclosan
high performance liquid chromatography
examination
