摘要
建立了反相高效液相色谱法测定饮料中苯甲醛的方法。当苯甲醛的质量浓度在1．0～100．0 mg·L-1范围时,苯甲醛的浓度与色谱峰面积呈线性关系,线性相关系数为0．999 8。苯甲醛的回收率为99．3%-102．6％,相对标准偏差为2．0%～3．4%,方法的检出限为0．1 mg·kg-1。
RP-HPLC was applied to the determination of benzaldehyde in drinks. Linearity was kept between the peak area of the chromatogram of benzaldehyde and its concentration in the range of 1.0- 100. 0 mg · kg^-1 （r=0. 999 8）, with a detection limit of 0. 1 mg · kg^-1. Tests for precision and recovery were carried at 3 concentration levels, i.e. 10. 0, 50.0 and 100.0 mg · kg^-1, values of RSD＇s （n=6） obtained were in the range of 2.0%-3.4%, and values of recoveries were in the range from 99.3%-102. 6%.
出处
《理化检验（化学分册）》
CAS
CSCD
北大核心
2006年第11期921-922,共2页
Physical Testing and Chemical Analysis(Part B:Chemical Analysis)
