期刊文献+
任意字段
题名或关键词
题名
关键词
文摘
作者
第一作者
机构
刊名
分类号
参考文献
作者简介
基金资助
栏目信息

大尺度Co_9S_8纳米线超声喷雾热解制备 被引量：1

Synthesis of the Wide Co_9S_8 Nanowires
下载PDF
导出
摘要 以CoC l2.6H2O和CS(NH2)2为先驱物,运用超声喷雾热解法在300℃的玻璃衬底上成功地制备了Co9S8纳米线,所得Co9S8纳米线的直径约为500 nm.利用X射线衍射(XRD)、光学显微镜分别对产物的物相和形貌进行了表征,同时讨论了产生大尺度纳米线的软模板机理. Co9S8 nanowires were synthesized using cobalt chloride （CoC12 . 6H2O） and thiourea （CS（ NH2 ）2 ） as the starting materials with the spray pyrolysis method on glass substrate at 300% with the diameter of about 500nm. The Co9S8 samples were characterized by X-ray diffraction （XRD） and optical microscope respectively, and a soft template principle was discussed for the formation of the wide Co9S8 nanowires.
作者 殷鹏飞 王声乐
机构地区 东南大学物理系
出处 《南京师范大学学报（工程技术版）》 CAS 2006年第4期50-52,共3页 Journal of Nanjing Normal University(Engineering and Technology Edition)
基金 江苏省自然科学基金资助项目(BK2004076)
关键词 Co9S8 纳米线 喷雾热解 Co9S8, nanowires, spray pyrolysis
分类号 TB383 [一般工业技术—材料科学与工程]
  • 相关文献

参考文献10

  • 1[1]WOLD A,DWIGHT K.Solid State Chemistry[M].New York:Chapman & Hall Inc,1993.
  • 2[2]CHAUKE H R,NGUYEN-MANH D,NGOEPE P E,et al.Electronic structure and stability of the pentlandites Co9S8 and (Fe,Ni)9S8[J].Phys Rev B,2002,66(15):155 105(5).
  • 3[3]IGOR B,PAVEL A,MICHEL D.Preparation of highly dispersed pentlandites (M,M')9S8 (M,M'=Fe,Co,Ni) and their catalytic properties in hydrodesulfurization[J].J Phys Chem B,2004,108(23):7 709-7 715.
  • 4[4]YAMADA H,TERAO K,AOKI M.Electronic structure and magnetic properties of CoS2[J].J Magn Magn Mater,1998,177-181(Part1):607-608.
  • 5[5]SCHNEEMEYER L F,SIENKO M J.Crystal data for mixed-anion molybdenum dichalcogenides[J].Inorg Chem,1980,19(3):789-791.
  • 6[6]PASQUARIELLO D M,KERSHAW R,PASSARETTI J D,et al.Low-temperature synthesis and properties of Co9S8,Ni3S2,and Fe7S8[J].Inorg Chem,1984,23(7):872-874.
  • 7[8]LIU X H.Hydrothermal synthesis and characterization of nickel and cobalt sulfides nanocrysta-llines[J].Mat Sci Eng B,2005,119(1-3):19-24.
  • 8[9]WANG S Y,WANG W,LU Z H.Asynchronous-pulse ultrasonic spray pyrolysis deposition of CuxS(x=/1,2) thin films[J].Mater Sci Eng B,2003,103(2):184-188.
  • 9[10]WANG W,WANG S Y,LIU M.Preparation of γ-Gd2S3films by ultrasonic spray pyrolysis[J].Mater Chem Phys,2005,94(2-3):182-184.
  • 10[11]WANG W,WANG S Y,LIU M.Growth of rod-like crystal BiSI films by ultrasonic spray pyrolysis[J].Mater Res Bull,2005,40(10):1 781-1 786.

同被引文献20

  • 1杨福宝,卢彩涛,胡强,贺会军,徐骏,石力开.超声雾化Sn-Pb焊锡粉的组织特征及其抗氧化性能[J].稀有金属,2005,29(6):832-836. 被引量：6
  • 2张嘉琪,谢秀荣,董迎.基于超声波雾化技术制备纳米TiO_2粉体及其表征[J].天津理工大学学报,2006,22(2):46-49. 被引量：4
  • 3邓新荣,胡国荣,彭忠东,曹雁冰.喷雾热解法合成球形(Y,Gd)BO_3:Eu荧光粉的研究[J].中国稀土学报,2007,25(2):167-171. 被引量：5
  • 4王登志,殷鹏飞,王声乐.超声喷雾热解法制备Co_9S_8纳米球壳[J].南京师范大学学报（工程技术版）,2007,7(3):52-55. 被引量：1
  • 5Jokanovic V, Janackovic D, Uskokovic D. Influence of aerosol formation mechanism by an ultrasonic field on particle size distribution of ceramic powders [ J ]. Ultrasonics Sonochemistry, 1999,6 (3) :157 -169.
  • 6Camelot D, Marijnissen J C M, Scarlett B. Production of metal oxide particles using the spray pyrolysis process [ J ]. Journal of Aerosol Science, 1996,27( 1 ) :403 -404.
  • 7Padmanabhan P V A,Ramanathan S,Sreekumar K P,et al. Synthesis of thermal spray grade yttrium oxide powder and its application for plasma spray deposition [ J ]. Materials Chemistry and Physics, 2007,106 (2/3) :416 - 421.
  • 8Stopic S, llic I, Uskokovic D. Structural and morphological transformations during NiO and Ni particles generation from chloride precursor by ultrasonic spray pyrolysis [ J ]. Materials Letters, 1995,24 (6) :369-376.
  • 9Che S L,Takada K,Yakashima K. Preparation of dense spherical Ni particles and hollow NiO particles by spray pyrolysis [ J ]. J. mater. Sic. ,1999,34:1313 - 1318.
  • 10Seiichi Suda, Seiji Takahashi, Mitsunobu Kawano, et al. Effects of atomization conditions on morphology and SOFC anode performance of spray pyrolyzed NiO- Smo.2Ce0.8O1.9 composite particles [ J]. Solid State Ionics,2006,177 ( 13 ) : 1219 - 1225.

引证文献1

二级引证文献2

南京师范大学学报（工程技术版）
2006年 第4期

相关作者

内容加载中请稍等...

相关机构

内容加载中请稍等...

相关主题

内容加载中请稍等...

浏览历史

内容加载中请稍等...
;
使用帮助 返回顶部