摘要
采用Ca（NO3）2·4H2O-P2O3-NH4F-乙醇体系，借助溶胶凝胶法在不同引氟量时制备了含氟羟基磷灰石（FHA，Ca10（PO4）6（0H）（2-x）Fx，x=0-2）纳米粉体，并利用XRD、IR和TEM对制备的粉体进行表征。结果表明：随引氟量的改变，FHA粉体的晶格常数、晶粒尺寸和显微结构等均呈现一定规律地变化。其中，晶格常数随着F引入量的增加逐渐减小，而晶粒尺寸却随之增大。
Nano-fluor-hydroxyapatite （ Ca10 （ PO4 ） 6 （ OH ）（2-x） Fx, x = 0-2, FHA） powders with different fluorine content were obtained by sol-gel using Ca （NO3）2 · 4H2O-P2O5·NH4F-alcohol system. The powders were measured by X-ray diffraction （XRD）, fourier transmission infrared spectrum （FT-IR） and transmission electron microscopy （TEM）, respectively. The resuhs indicate that lattice parameter, grain size and microstructure of the heat-treated powders varied regularly corresponding to the fluoride addition. For example, the lattice parameter decreased while grain size increased with fluoride addition increasing.
出处
《硅酸盐通报》
CAS
CSCD
北大核心
2006年第6期1-4,共4页
Bulletin of the Chinese Ceramic Society
基金
国家自然科学基金资助课题(No.50372037)
