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新型二氮冠醚臂式衍生物的合成与表征 被引量：2

THE SYNTHESES AND CHARACTERIZATION OF NEW ARMED-DIAZACROWN ETHER DERIVATIVES
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摘要 合成了对羟基苯甲酸乙酯双侧臂取代的二氮杂18-冠-6衍生物L1,在盐酸中水解得到了对羟基苯甲酸双侧臂取代的二氮杂18-冠-6衍生物L2,用元素分析、红外光谱和核磁共振谱对新大环化合物进行了表征. The new derivative of diazacrown ether with two ethyl parahydroxy benzoic acid ester side arms （L1） is designed and synthesized. L1 is hydrolyzed using hydrochloric acid and H2O （1： 1） and another derivative of diazacrown ether which contains two parahydroxybenzoic acid side arms （L2） is obtained. L1 and L2 have not been reported in other articles. Their structures are characterized by elemental analysis, ^1HNMR and IR spectra.
作者 王小珠 马淑兰 朱文祥 刘迎春 张静
机构地区 北京师范大学化学学院 北京师范大学图书馆
出处 《北京师范大学学报（自然科学版）》 CAS CSCD 北大核心 2006年第6期597-600,共4页 Journal of Beijing Normal University(Natural Science)
基金 北京师范大学青年基金资助项目(10770005)
关键词 二氮取代冠醚 羧基衍生物 合成 diazacrown ether carboxylic derivative synthesis
分类号 O636.1 [理学—高分子化学]
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参考文献10

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同被引文献21

  • 1赵明根,韩江华.多甘醇双对甲苯磺酸酯的最新合成方法[J].化学试剂,1994,16(1):50-50. 被引量：4
  • 2陈学刚,程延祥,耿延侯,王利祥.双核三联吡啶钌(Ⅱ)配合物的合成及其光谱和电化学性质[J].应用化学,2006,23(5):465-470. 被引量：7
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  • 4Ding Z J, Zhang Y M, Teng X, et al. Controlled photo- physical behaviors befween dibenzo-24-crown-8 bearing terpyridine moiety and fullerene-containing ammonium salt[J]. J Org Chem,2011,76(6) :1910 -1915.
  • 5Chung S K, Tseng Y R, Chen C Y, eta/. A selective colorimetric Hg2 probe featuring a styryl dithiaazacrown containing platinum (II) terpyridine complex through modulation of the relative strength of ICT and MLCT transitions [ J ]. Inorg Chem,2011,50 (7) :2711 - 2713.
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北京师范大学学报（自然科学版）
2006年 第6期

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