摘要
目的:建立轻宁胶囊的质量标准。方法:采用薄层扫描法对轻宁胶囊中的山楂、陈皮进行定性鉴别;采用高效液相色谱法测定金丝桃苷的含量。结果:薄层色谱鉴别特征斑点明显;金丝桃苷在0.3-1.5μg范围内线性关系良好(r=0.9993),平均回收率为100.2%(RSD=1.11%)。结论:轻宁胶囊质量可控制。
OBJECTIVE: To establish the quality criterion for Qingning capsules. METHODS: Rhizpma cyperi, pericarpium citri reticulatae in Qingning capsules were identified by TLC,The content of hyperoside was determined by HPLC. RESULTS: The TLC revealed clear spots in diagnostic characteristics. Hyperoside showed good linear relationship in the range of 0.3- 1.5μg(r = 0.999 3), with a recovery rate of 100.2% (RSD =1.11%) . CONCLUSION: The quality of Qingning capsules could be controlled.
出处
《中国药房》
CAS
CSCD
北大核心
2007年第3期211-213,共3页
China Pharmacy