摘要
以固体FeCl3.6H2O为催化剂催化合成苯甲酸丁酯,讨论了影响催化酯化的各种因素。其优化的反应条件为:n(苯甲酸)∶n(丁醇)=1∶3.0、n(催化剂)∶n(苯甲酸)=0.04∶1、反应时间为2.0 h,此时苯甲酸丁酯的产率约为90%。
The synthesis of butyl benzoate with ferric trichloride as catalyst was studied. The effects of reaction parameters were investigated and the optimum conditions were determined as follows： the molar ratio of benzoic acid to butanol 1 ： 3.0, the molar ratio of catalyst to benzoic acid was 0.04 ： 1, the reaction time was 2.0 h,and the yield of butyl benzoate was about 90%.
出处
《化学与生物工程》
CAS
2007年第1期34-35,共2页
Chemistry & Bioengineering
关键词
苯甲酸丁酯
三氯化铁
催化
合成
butyl benzoate
ferric chloride
catalysis
synthesis
