摘要
采用机械合金化方法,在摆振式高能球球磨机上制备Fe-Co-Nb-B纳米晶合金粉末,计算球磨后应力带来的晶格畸变对X射线衍射峰宽化的影响.样品有较高的比饱和磁化强度和矫顽力,在1 073 K烧结后,虽然消除了内应力的影响,但也使晶粒尺寸有所长大.
The Fe-Co-Nb-B nanocrystalline powders were mechanically alloyed with a vibrational high energy ball mill. The effect of lattice distortion on the broadening of X-ray diffraction peaks was calculated. Samples exhibit satisfactory saturation magnetization and high coercivity. The annealing process at 1 073 K can ease the local stress but also results in the coarsening of the crystal grains.
出处
《华侨大学学报(自然科学版)》
CAS
北大核心
2007年第1期51-54,共4页
Journal of Huaqiao University(Natural Science)
基金
福建省自然科学基金资助项目(2006J0451)
集美大学科研基金资助项目(C60514)
关键词
纳米晶
机械合金化
球磨
软磁材料
nanocrystalline
mechanical alloying
ball mill
soft magnetic material