摘要
目的:建立骨疽康膏的质量标准。方法:采用薄层色谱法对制剂中的当归、川芎、血竭、独活、羌活进行鉴别;采用气相色谱法测定制刑中麝香酮的含量。结果:在薄层色谱中以当归、川芎、羌活、血竭、独活为对照药材,能较好地鉴别出制剂中的当归、川芎、羌活、血竭、独活。气相色谱法能准确地测定出制剂中麝香酮的含量,麝香酮进样量在0.3064~1.5320μg范围内线性关系良好,r=0.998,平均加样回收率为99.418%。结论:此方法简单可行,能快速准确地对骨疽康膏进行鉴别和含量测定。
Objective: To establish the quality standard of Gujukang Extract. Methods: Danggui, Chuanxong, Xuejie, Duhuo, Qianghuo were identified by TLC, and the content of Muskone was determined by GC. Results: Danggui, Chuanxong, Xuejie, Duhuo, Qianghuo could be identified Well by TLC. Muskone showed a good linear relation.ship at range of 0. 3064-1. 5320 μg, r= 0. 998, The average recovery was 99. 418%. Conlusion: The method is accurate and can be used to control the quality of Gujukang Extract.
出处
《河南中医学院学报》
2007年第1期51-52,共2页
Journal of Henan University of Chinese Medicine
关键词
骨疽康膏
质量标准
麝香酮
气相色谱法
Gujukang Extract
Quality Standard
Muskone
The Gas Chromatography