摘要
改进了Ｎ－（４－异硫氰基丁基）－Ｎ－乙基异鲁米诺的合成路线，设计了制备Ｎ－甲基－４－硝基邻苯二甲酰亚胺的新方法，对某些制备反应的条件进行了优化。
The synthesis route for ITCBEI is improved, and a new synthetic method for N-methyl-4-nitrophthalimide is designed. Reaction conditions for some intermediates are investigated. As a result, some intermediates yieleds and total yieleds for ITCBEI are raised.
出处
《福州大学学报（自然科学版）》
CAS
CSCD
1996年第5期91-94,共4页
Journal of Fuzhou University(Natural Science Edition)
基金
国家自然科学基金
福建省属高等院校测试基金
关键词
化学发光
免疫分析试剂
ITCBEI
chemiluminescence
immunoassay reagent
N-(4-isothiocyanatobutyl)-N-ethylisoluminol
N-methyl-4-nitrophthalimide
synthesis
