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苯炔前体邻-三甲硅基苯酚三氟甲磺酸酯的合成 被引量：3

Synthesis of Aryne Precursor o-Trimethylsilylphenyl Triflate
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摘要 以邻溴苯酚为起始原料,经硅基化、水解和酯化反应得到苯炔前体邻-三甲硅基苯酚三氟甲磺酸酯,总收率75%。其结构经1HNMR,13CNMR,19FNMR和IR表征。 o-Trimethylsilylphenyl triflate was synthesized from o-bromophenol by silylation, hydrolysis and esterification reaction in total yield of 75%. The structure was characterized by ^1H NMR, ^13C NMR, ^19F NMR and IR.
作者 仵清春 李保山 石常青 陈彦逍
机构地区 北京化工大学理学院 中国科学院成都有机化学研究所
出处 《合成化学》 CAS CSCD 2007年第1期111-113,共3页 Chinese Journal of Synthetic Chemistry
关键词 邻溴苯酚 硅基化 苯炔前体 o-bromophenol silylation aryne precursor
分类号 O625.75 [理学—有机化学]
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参考文献20

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共引文献10

同被引文献89

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合成化学
2007年 第1期

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