摘要
以糠醛为起始原料,通过康尼查罗反应、酰氯化和酯化反应合成了糠酸甲酯,实验结果表明:酯化反应时间2.5h,糠酸甲酯收率可达85.0%。
Methyl-furoate is synthesized from furfural by Cannizzaro reaction, acyl chloride reaction and esterification. It showed that the time of esterification is only 2.5 hours and the yield can reach 85.0%.
出处
《精细化工中间体》
CAS
2007年第1期41-42,45,共3页
Fine Chemical Intermediates
关键词
糠酸甲酯
糠醛
二氯亚砜
康尼查罗反应
酯化
methyl-furoate
furfural
sulfuryl dichloride
cannizzaro reaction
esterification
