摘要
目的建立首乌芪灵胶囊的质量控制方法。方法薄层色谱法(TLC)鉴别制剂中何首乌、黄芪、淫羊霍和紫河车;高效液相色谱法(HPLC)测定何首乌的主要成分2,3,5,4'-四羟基二苯乙烯-2-O-β-D-葡萄糖苷(二苯乙烯苷)的含量。结果定性鉴别方法重现性好,专属性强;二苯乙烯苷的回收率为100.13%,RSD为0.85%。结论方法操作简便,快速,准确,能够有效地控制首乌芪灵胶囊的质量。
Aim To establish a method for nalysis of Radix Polygoni Multiflori , Radix As quality control of Shouwuqiling Capsule. Methods The qualitative atragali , Herba Epimedii, Placenta Hominis in Shouwuqiling Capsule was identifed by TLC. The content of 2,3,5,4'-tetrahydroxystilbene -2-O-β-D- glucoside in the capsule was determinated by HPLC. Results Methods of the qualitative identifications were specific and reproducible. The average recoyery of 2,3,5,4 '-tetrahydroxystilbene-2-O-β-D-glucoside was 100.13 % and RSD = 0.85 % ( n = 9 ). Conclusion This method is simple and accurate and can be effectively used for controlling the quality of Shouwuqiling Capsule.
出处
《解放军药学学报》
CAS
2007年第1期51-54,共4页
Pharmaceutical Journal of Chinese People's Liberation Army
基金
福建省科技攻关计划重点资助项目
No.2002Y022
关键词
首乌芪灵胶囊
TLC鉴别
二苯乙烯苷
HPLC
Shouwuqiling Capsule
TLC
HPLC
2,3,5,4'-tetrahydroxystilbene-2-0-13-D- glueoside