两种N-硝基取代苯胺的制备

Synthesis of Two Substituted Phenylnitramine

以邻硝基苯胺、对硝基苯胺为原料,乙酰硝酸酯作硝化剂,合成两种N-硝基取代苯胺类化合物,产率分别为71.03%和60.1%,产物经IR、1H NMR、质谱、元素分析表征。

Two substituted phenylnitramines were prepared by nitration of ortho- and para-nitro aniline with acetyl nitrate. The rate of yields was 71.03% and 60.1%. Their structures were confirmed by IR, ^1H NMR, MS spectra and elemental analyses.