摘要
根据氯苯在水体中溶解度小，易吹脱且热稳定性好的特点，建立了水体中痕量氯苯的分析方法。该法采用简化的吹脱、捕集装置用ＴｅｎａｘＧＣ富集水体中氯苯，热解吸法浓缩进样，大口径毛细管柱分离，ＦＩＤ测定。方法操作简单、快速，测定水体中氯苯最低检出限为０．４μｇ／Ｌ，相对标准偏差小于８．６％。
A rapid and reliable gas chromatographic method for determining trace phylchloried in water is presented.The analytical procedures are as follows:concentration with simplified parge and trap,thermal desorption at 200℃,separation with HP 20M capillary column and determination by FID.The detection limit is 0 4μg/L.The proposed method has been applied to determine water samples with satisfactory result.
出处
《中国环境监测》
CSSCI
CSCD
北大核心
1996年第6期16-19,共4页
Environmental Monitoring in China
关键词
水质监测
氯苯
气相色谱法
trace phylchloride,parge and trap,thermal desorption
