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Keggin结构的钨钴杂多酸盐的合成与表征 被引量：3

Synthesis and Characterization of Tungstocobalt Heteropoly Salts Having keggin Structure
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摘要 本文以钨酸钠和硝酸钴为原料合成了钨钴杂多酸盐。利用红外光谱、差热分析、可见紫外分光光度法和循环伏安法研究了其结构类型、分解脱水温度和氧化还原性质以及酸度对氧化还原性质的影响。 Tungstocobalt heteropoly salts were synthesized using sodium tungstate and cobalt nitrate as materials. Type of structure, temperatures of decomposition and dehydration, redox properies and pH related redox properties were studied by IR spectra,DTA, UV-visible spectra and cyclic voltammetty.
作者 霍国燕
出处 《河北大学学报（自然科学版）》 CAS 1996年第1期42-47,共6页 Journal of Hebei University(Natural Science Edition)
关键词 KEGGIN结构 钨钴杂多酸盐 合成 表征 红外光谱 Keggin structure Tungstocobalt heteropoly salts Sythesis Characterization
分类号 O641.4 [理学—物理化学]
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参考文献1

  • 1[美]安森(F·Amsom) 讲授,黄慰曾等.电化学和电分析化学[M]北京大学出版社,1983.

同被引文献16

  • 1高丽华,王科志.具有Keggin和Dawson结构的钨钼杂多阴离子的有机衍生物及其应用[J].化学通报,1993(12):40-45. 被引量：15
  • 2FRED BASOLO, RONALD C. JOHNSON. Coordination Chemistry[ M]. Menlo Park, California: W A BENJAMIN INC, 1982.
  • 3SARAH J DUNNE, ROBERT C BURNS, GEOFFREY A LAWRANCE. Oxidation of nickel ( Ⅱ) and manganese (Ⅱ) by peroxodisulfate in aqueous solution in the presence of molybdate: crystal structure of the (NH4)6 [NiMo9O32 ]6H2O product[J]. Aust J Chem, 1992, 45: 1943- 1952.
  • 4SARAH J DUNNE, ROBERT C BURNS, TREVOR W HAMBLEY, et al. Oxidation of manganese (Ⅱ) by peroxomonosulfuric acid in aqueous solution in the presence of molybdate: crystal structure of the K6 [ MnMo9O32 ] 6H2O product [J ]. Aust J Chem, 1992, 45: 685- 693.
  • 5Arslan I,Bacdglu A.Oxidative treatment of simulated dye house by UV and near-UV light assisted Fenton′s reagent[J].Chemosphere,1999,39(15):2767-2783.
  • 6Chu W,Ma C.Reaction kinetics of UV decolourization for dye materials[J].Chemosphere,1998,37(5):961-974.
  • 7Wu Feng,Deng Nan-heng,Hua He-lin.Degradation mechanism of azo dye C.I.reactive red 2 by iron powder reduction and photooxidation in aqueous solutions[J].Chemosphere,2001,41:1233-1238.
  • 8Tui S,Chu W.Quantum yield study of the photodegradation of hydrophobic dyes in the presence of acetone sensitizer[J].Chemosphere,2001,44:17-22.
  • 9Hu Mei-qin,Xu Yi-ming.Photocatalytic degradation of textile dye X3B by heteropolyoxometallate acids[J].Chemosphere,2004,54:431-434.
  • 10Annette L N,Robert C B,Geoffrey A L.Oxidation of[Co^ⅡW12O40]^6-to[Co^ⅢW12O40]^5 by peroxomonosulfate in strong and weak acid solutions,an example of zero-order kinetics[J].J Chem Soc Dalton Trans,1998(5):3041-3047.

引证文献3

二级引证文献16

河北大学学报（自然科学版）
1996年 第1期

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