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GC-MS法测定青岛海滨海水中的有机锡 被引量:17

DETERMINATION OF ORGANOTIN COMPOUNDS IN SEAWATER OF QINGDAO BEACH BY GC-MS
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摘要 采用GC-MS方法监测青岛海滨海水中的有机锡污染情况。对有机锡测定的衍生化条件进行了优化,GC-MS方法对青岛海滨海水中的有机锡的污染现状及形态分布进行了调查,结果表明青岛六个取样点的海水中都存在着有机锡不同程度的污染。 The determination of organotin compounds in seawater of Qingdao beach using gas chromatography-mass spectrometry(GC-MS) is described. The method involves extraction of organotin compounds from seawater with CH2Cl2 and drivatization with NaBEt4. Then the ethyl organotin were analyzed by GC/MS in the selective ion mode. Based on our investigation, the contamination resulted from organotin compounds can be concluded.
出处 《海洋湖沼通报》 CSCD 北大核心 2007年第1期62-68,共7页 Transactions of Oceanology and Limnology
关键词 有机锡 海水 测定 organotin seawater determination
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