空气氧化法合成均苯三甲酸过程中的产物分析

Analysis of Final Products in Composition of Trimesic Acid by Catalytic Oxidation Method

针对均三甲苯气液相催化空气氧化合成均苯三甲酸的反应及相关的工艺过程中,反应产物均苯三甲酸的分析问题,提出以色谱分析、质谱分析、红外光谱分析、原子吸收光谱分析及化学滴定为主要分析手段对反应组分进行分析,重点研究并建立了相关的分析方法。

In the gas-liquid phase reaction of catalytic oxidation of mesitylene by air to synthesize trimesic acid and the related process, an analysis method of reaction components was proposed, which includes chromatographic analysis, mass spectral analysis, IR spectrum, atomic absorption spectrophotometer and chemical titration for the purpose of analyzing reaction groups. The stress was on this particular research, with relevant analyzing method built.