摘要
选用不同的醇改性剂,在自制的直链淀粉-三(3,5-二甲基苯基氨基甲酸酯)(ADMPC)手性固定相上,对2种吲哚环衍生物对映体进行了手性拆分研究,并考察了样品的保留时间和立体选择性.
Two enatiomers of indole ring derivatives have been chiral separated on amylase-tris （3, 5- dimethylphenylcarbamate） chiral stationary phase （CSP）, using hexane as the mobile phase with various alcohols as modifiers. The influence of the mobile phase composition on the enantioselectivity was discussed. By comparing the results from amylase-tris （3,5- dimethylphenylcarbamate） chiral stationary phase and cellulose tris （3, 5- dimethylphenylcarbamate） chiral stationary phase, the separation abilities are different on the two stationaries.
出处
《分析测试技术与仪器》
CAS
2007年第1期30-32,共3页
Analysis and Testing Technology and Instruments
