利用电流积分器和峰值保持单元改进固体电极上的多重峰测量和提高记录仪记录伏安图的精确性

Improving the accuracy and Reliability of Recorded Voltammogram by the Current Integrator and Peak Height Detector

本文推荐采用电流积分器和峰值保持(检测)器作为插入单元,以测量积分电量代替峰高测量,改进固体电极上的测量浓度范围。并采用峰值检测器提高记录仪的响应,使之适用于500～1000mV/s扫描速率下的伏安测定。本文以T(Ⅳ)作为例子证明上述优点。

A current integrator and a peak height detector are proposed as an interposed unit sothat the readout of stripping coulometry being used instead of the peak current when the latter gives multiple waves, and a peak maximun being kept to ensure good precision of recorder. The determination of telluiium(IV)demonstrates the readout reliablity of recorder on voltammogram being significantly improved.