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Synthesis and characterization of nanocrystalline Ni produced by cryomilling in liquid nitrogen 被引量:2

Synthesis and characterization of nanocrystalline Ni produced by cryomilling in liquid nitrogen
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摘要 NanocrystaUine Ni powders were successfully fabricated by mechanically milling at cryogenic temperature (cryomilling) with 1 wt.%Y2O3 particles. The experimental results have shown that the Ni grain size is reduced to 25 nm after 2 h of cryomilling in the presence of the Y2O3 particles. The cryomiUed Ni/Y2O3 powders can maintain their nanocrystalline structure up to 900℃, or 62% of the melting point of Ni. A bulk nanocrystalline Ni/Y2O3 material with a thermally stable grain size of approximately 100 nm was produced by cryomilling, cold isostatic pressing, followed by hot isostatic pressing. The microhardness of bulk nanocrystalline Ni/1wt.%Y2O3 is 315 DPH, which is two times as high as that of conventional Ni. NanocrystaUine Ni powders were successfully fabricated by mechanically milling at cryogenic temperature (cryomilling) with 1 wt.%Y2O3 particles. The experimental results have shown that the Ni grain size is reduced to 25 nm after 2 h of cryomilling in the presence of the Y2O3 particles. The cryomiUed Ni/Y2O3 powders can maintain their nanocrystalline structure up to 900℃, or 62% of the melting point of Ni. A bulk nanocrystalline Ni/Y2O3 material with a thermally stable grain size of approximately 100 nm was produced by cryomilling, cold isostatic pressing, followed by hot isostatic pressing. The microhardness of bulk nanocrystalline Ni/1wt.%Y2O3 is 315 DPH, which is two times as high as that of conventional Ni.
出处 《Rare Metals》 SCIE EI CAS CSCD 2007年第2期147-151,共5页 稀有金属(英文版)
基金 This project was financially supported by the High Technical Research and Development Programme of China (No. 2002AA302502).
关键词 NANOCRYSTALLINE mechanical milling NICKEL CHARACTERIZATION nanocrystalline mechanical milling nickel characterization
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