摘要
研究了合成对甲苯基氯化汞的方法,考察了反应物料比、反应温度等对合成的影响,给出了合成的最佳反应条件。产物经各项参数和谱图鉴定,在最佳反应条件下,产率达到了94%,纯度为99.9%。
The synthesis method of p-menthylphenyl mercuric chloride was carried out. The effect of reactant ratio, reaction temperature were investigated and the optimal reaction conditions were also confirmed sequentially. Under the optimal reaction conditions, the yield and purity were 94 %, 99.9 % respectively.
出处
《广州化工》
CAS
2007年第2期27-28,共2页
GuangZhou Chemical Industry
关键词
有机合成
有机金属化合物
对甲苯基氯化汞
重氮化
organic synthesis
organometallic compounds
p-menthylphenyl mercuric chloride
diazonium reaction